 Sample mix of 3 penta-decapeptides as shown above. Single spiral rotor in 1%Tfa
/sec-butanol in elution mode L-i-T, 800 rpm, 2
ml/min. Sf = 88%. HPLC analysis of fractions. HPLC with 0.1%Tfa/acetonitrile gradient with C-18
column. Note order of elution of two
peptides different in HPLC. Synthetic
peptides have been purified in up to 100-mg amounts in single spiral and STS
rotors. Results are in publications
listed. |  |
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